HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piconol → HCID 9944478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piconol | HCID 11474 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 18507414 | HCID 18507414 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 9944478 | HCID 9944478 | — |
Reaction Steps
From 2-amino-4-methanesulfinyl-6-thiophen-2-yl-pyrimidine-5-carbonitrile, 2-(hydroxymethyl)pyridine and DBU in dioxane. EI-MS m/e (%): 309 (M+, 53), 308 ([M—H]+, 48), 292 ([M—NH3]+, 32), 108 (100), 92 (50), 65 (49).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-83e49589b1d044d4a464fb64b752523d |
| Source note | uspto-grants-2003_07 |