Ethylamine → HCID 18507237, compound

HRID 1355889Notes

Reaction equation

HRID 1355889 reaction equation

[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[CH2:17]([NH2:19])[CH3:18]>C1COCC1>[Br:1][C:2]1[C:7]([NH:19][CH2:17][CH3:18])=[N:6][C:5]([NH2:11])=[N:4][C:3]=1[C:12]1[O:13][CH:14]=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 6341Ethylamine

HCID 185072865-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine

Product 1

HCID 18507237HCID 18507237, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine and ethylamine in THF. ES-MS m/e (%): 285 (M{81Br}+H+, 100), 283 (M{79Br}+H+, 95).

Sources & evidence

ORD record: ord-2abeef48232242f0b7f2afaf7acf50d7
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06586441B2

Reaction notes

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