HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → HCID 18507489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 5-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine | HCID 18507286 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18507489 | HCID 18507489 | — |
Reaction Steps
From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, benzylmercaptan and DBU in dioxane. EI-MS m/e (%): 363 (M{81Br}+, 48), 361 (M{79Br}+, 46), 282 ([M—Br]+, 68), 249 (35), 91 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-d7e40acadddd4b44a3465bb9a2ef0ad0 |
| Source note | uspto-grants-2003_07 |