HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanethiol → HCID 18507381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanethiol | HCID 8012 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 5-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine | HCID 18507286 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18507381 | HCID 18507381 | — |
Reaction Steps
From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, butanethiol and DBU in dioxane. EI-MS m/e (%): 329 (M{81Br}+, 29), 327 (M{79Br}+, 28), 287 ([M{81Br}-C3H6]+, 46), 285 ([M{79Br}—C3H6]+, 45), ), 273 ([M{81Br}—C4H8]+, 98), 271 ([M{79Br}—C4H8]+, 99), 248 ([M—Br]+, 54), 206 (100), 192 (34), 117 (34).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-7319994e01384a47b41057df33dc65cc |
| Source note | uspto-grants-2003_07 |