Methylamine → HCID 18507542, compound

HRID 1355928Notes

Reaction equation

HRID 1355928 reaction equation

[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[C:11]([I:12])=[C:10](S(C)=O)[N:9]=[C:8]([NH2:16])[N:7]=1.[CH3:17][NH2:18]>C1COCC1.C(O)C>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[N:7]=[C:8]([NH2:16])[N:9]=[C:10]([NH:18][CH3:17])[C:11]=1[I:12]

Participants

4

Reactant 2

HCID 6329Methylamine

HCID 18507211HCID 18507211, compound

Product 1

HCID 18507542HCID 18507542, compound

Reagents, catalysts & solvents 1

HCID 21873804Tetrahydrofuran ethanolSolvent

Procedure

From 4-furan-2-yl-5-iodo-6-methanesulfinyl-pyrimidin-2-yl-amine and methylamine in THF/ethanol. ES-MS m/e (%): 317 (M+H+, 100).

Sources & evidence

ORD record: ord-27d81a429c8749138eefb217cdb3d637
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06586441B2

Reaction notes

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