Cyclohexanol → HCID 18507521, compound

HRID 1355945Notes

Reaction equation

HRID 1355945 reaction equation
[NH2:1][C:2]1[C:7]([C:8]#[N:9])=[C:6]([C:10]2[O:11][CH:12]=[CH:13][CH:14]=2)[C:5]([C:15]#[N:16])=[C:4](S(C)=O)[N:3]=1.[CH:20]1([OH:26])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1.C1CCN2C(=NCCC2)CC1>COCCOC>[NH2:1][C:2]1[C:7]([C:8]#[N:9])=[C:6]([C:10]2[O:11][CH:12]=[CH:13][CH:14]=2)[C:5]([C:15]#[N:16])=[C:4]([O:26][CH:20]2[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]2)[N:3]=1

Participants

5

Reactant 3

HCID 7966CyclohexanolHCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 18507288HCID 18507288, compound

Product 1

HCID 18507521HCID 18507521, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-furan-2-yl-6-methanesulfinyl-pyridine-3,5-dicarbonitrile, cyclohexanol and DBU in DME. EI-MS m/e (%): 308 (M+, 12), 226 ([M—C6H10]−, 100).

Sources & evidence

ORD record
ord-96a165725bfb44e4b3f7b89038112990
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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