Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1355947Generated: November 1, 2026

1-Butanol → HCID 18507457, compound

https://huagongshe.com/reaction/1355947

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-ButanolHCID 263—
Reactant1,8-Diazabicyclo(5.4.0)undec-7-eneHCID 81184—
ReactantTrifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl esterHCID 86583748—
Solvent1,2-DimethoxyethaneHCID 8071—
ProductHCID 18507457HCID 18507457—

Reaction Steps

From trifluoro-methanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester, butanol and DBU in DME. EI-MS m/e (%): 278 (M+, 24), 249 ([M—C2H5]+, 28), 193 (70), 177 (100), 150 (48), 108 (86), 94 (62), 70 (48), 69 (46), 43 (68), 41 (62), 29 (45).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06586441B2
Source datasetuspto-grants-2003_07
ORD IDord-f1b4e60066034d5c8c226a238eda1cbd
Source noteuspto-grants-2003_07