Methylamine → HCID 18507275, compound

HRID 1355951Notes

Reaction equation

HRID 1355951 reaction equation

[NH2:1][C:2]1[N:7]=[C:6](OS(C(F)(F)F)(=O)=O)[C:5]([N+:16]([O-:18])=[O:17])=[C:4]([C:19]2[O:20][CH:21]=[CH:22][CH:23]=2)[N:3]=1.[CH3:24][NH2:25]>COCCOC>[O:20]1[CH:21]=[CH:22][CH:23]=[C:19]1[C:4]1[N:3]=[C:2]([NH2:1])[N:7]=[C:6]([NH:25][CH3:24])[C:5]=1[N+:16]([O-:18])=[O:17]

Participants

4

Reactant 2

HCID 6329Methylamine

HCID 86583748Trifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester

Product 1

HCID 18507275HCID 18507275, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From trifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester and methylamine in DME. ES-MS m/e(%): 236 (M+H+, 100).

Sources & evidence

ORD record: ord-f8474dda3d9e48a793fd8f2297365854
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06586441B2

Reaction notes

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