Phenethylamine → HCID 18507614, compound

HRID 1355987Notes

Reaction equation

HRID 1355987 reaction equation
[Cl:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[CH2:17]([NH2:25])[CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>O1CCOCC1>[Cl:1][C:2]1[C:7]([NH:25][CH2:17][CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[N:6][C:5]([NH2:11])=[N:4][C:3]=1[C:12]1[O:13][CH:14]=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 1001PhenethylamineHCID 18507343HCID 18507343, compound

Product 1

HCID 18507614HCID 18507614, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

From 5-chloro-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine and phenethylamine in dioxane. ES-MS m/e (%): 317 (M{37Cl}+H+, 30), 315 (M{35Cl}+H+, 100).

Sources & evidence

ORD record
ord-e36a77127d854d028b7024e101c957d1
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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