1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 18507423, compound

HRID 1356074Notes

Reaction equation

HRID 1356074 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[CH:11]=[C:10]([S:12]([CH3:14])=O)[N:9]=[C:8]([NH2:15])[N:7]=1.SC[CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=1.C1CCN2C(=NCCC2)CC1>COCCOC>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[CH:11]=[C:10]([S:12][CH2:14][CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=2)[N:9]=[C:8]([NH2:15])[N:7]=1

Participants

5

Reactant 3

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 1509632-PyridineethanethiolHCID 185072094-Furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine

Product 1

HCID 18507423HCID 18507423, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, 2-mercaptoethylpyridine and DBU in DME. ES-MS m/e (%): 299 (M+H+, 100), 194 (98), 106 (70).

Sources & evidence

ORD record
ord-eca5066c20d84488987eca625f157625
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

Loading…