1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 10224382, compound

HRID 1356096Notes

Reaction equation

HRID 1356096 reaction equation
[C:1]([C:3]1[C:4]([C:21]2[O:22][CH:23]=[CH:24][CH:25]=2)=[N:5][C:6]([NH:12][C:13](=[O:20])[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[N:7][C:8]=1[S:9]([CH3:11])=O)#[N:2].[N:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[CH2:32]CS.C1CCN2C(=NCCC2)CC1>COCCOC>[C:1]([C:3]1[C:4]([C:21]2[O:22][CH:23]=[CH:24][CH:25]=2)=[N:5][C:6]([NH:12][C:13](=[O:20])[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[N:7][C:8]=1[S:9][CH2:11][CH2:32][C:27]1[CH:28]=[CH:29][CH:30]=[CH:31][N:26]=1)#[N:2]

Participants

5

Reactant 3

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 1509632-PyridineethanethiolHCID 18507236HCID 18507236, compound

Product 1

HCID 10224382HCID 10224382, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From N-(5-cyano-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl)-benzamide, 2-pyridylethylmercaptan and DBU in DME. ES-MS m/e (%): 428 (M+H+, 100).

Sources & evidence

ORD record
ord-62e7d57531a94ad88835cece46ff19f5
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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