HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 18507465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 18507481 | HCID 18507481 | — |
| Reactant | 2-Amino-4-methanesulfinyl-6-pyridin-2-yl-pyrimidine-5-carbonitrile | HCID 18507695 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 18507465 | HCID 18507465 | — |
Reaction Steps
From 2-amino-4-methanesulfinyl-6-pyridin-2-yl-pyrimidine-5-carbonitrile, 2-aminomethyl-3-chloro-6-(trifluoromethyl)pyridine hydrochloride and DBU in DME. ES-MS m/e (%): 408 (M{37Cl}+H+, 25), 406 (M{35Cl}+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-aa1854b5aa4f4de8ac4b8b45248e0b06 |
| Source note | uspto-grants-2003_07 |