HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → 2-Amino-4-(4-iodo-pyrazol-1-yl)-6-methylsulfanyl-pyrimidine-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 4-Iodopyrazole | HCID 77022 | — |
| Reactant | 2-Amino-4-bromo-6-methylsulfanyl-pyrimidine-5-carbonitrile | HCID 18753230 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | 2-Amino-4-(4-iodo-pyrazol-1-yl)-6-methylsulfanyl-pyrimidine-5-carbonitrile | HCID 18507698 | — |
Reaction Steps
From 2-amino-4-bromo-6-methylsulfanyl-pyrimidine-5-carbonitrile, 4-iodopyrazole and cesium carbonate in NMP. EI-MS m/e (%): 359 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-fcdaf4ef7036457d8d0a2262d0ba38fc |
| Source note | uspto-grants-2003_07 |