HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 18507717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 4-Bromopyrazole | HCID 16375 | — |
| Reactant | 2-Amino-4-bromo-6-methylsulfanyl-pyrimidine-5-carbonitrile | HCID 18753230 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 18507717 | HCID 18507717 | — |
Reaction Steps
From 2-amino-4-bromo-6-methylsulfanyl-pyrimidine-5-carbonitrile, 4-bromopyrazole and cesium carbonate in NMP. EI-MS m/e (%): 313 (M{81Br}+H+, 95). 311 (M{79Br}+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-6b3b34a506764c3fa9764dbab05d9f33 |
| Source note | uspto-grants-2003_07 |