HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 18507291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 2-Pyridineethanethiol | HCID 150963 | — |
| Reactant | HCID 18507394 | HCID 18507394 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 18507291 | HCID 18507291 | — |
Reaction Steps
From 2-amino-4-(4-cyano-furan-2-yl)-6-methanesulfinyl-pyrimidine-5-carbonitrile, 2-mercaptoethylpyridine and DBU in DME. EI-MS m/e (%): 348 (M+, 90), 347 ([M—H]+, 65), 138 (100), 106 (70).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-b7ecd6de610a4dc2af621cf541f1edbc |
| Source note | uspto-grants-2003_07 |