HCID 22396816, compound → HCID 69893822, compound

Participants

Reaction Steps

Following the procedure for the preparation of 10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from 10-(3-chlorophenyl)-1,2,3,4,5,6-hexahydroazepino[4,5-b]indole dihydrochloride the title compound was prepared: 1H NMR (DMSO-d6) δ 1.35, 1.55, 2.10, 2.71, 3.05, 3.28, 3.97, 4.20, 6.65, 7.12, 7.4-7.5, 8.8. HRMS (FAB) calcd for C18H21ClN12 (MH+) 299.1315, found 299.1306.

Provenance & Evidence