HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22396943, compound → HCID 69894619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22396943 | HCID 22396943 | — |
| Reactant | HCID 22609212 | HCID 22609212 | — |
| Product | HCID 69894619 | HCID 69894619 | — |
Reaction Steps
Following the procedure for the preparation of 10-(4-chlorophenyl)-1,2,3,4,5,5a,6,10b-octahydroazepino[4,5-b]indole dihydrochloride, making non-critical variations, starting from 10-[3-(2-chlorophenoxy)propyl]-1,2,3,4, 5,6-hexahydroazepino[4,5-b]indole the title compound was prepared: 1H NMR (CDCl3) δ 1.99-2.20, 2.27, 2.78, 2.93-3.05, 3.51, 4.11, 6.48, 6.62, 6.92, 7.03, 7.19, 7.38, 7.40. HRMS (FAB) calcd for C21H25ClN2O1 (MH+) 357.1733, found 357.1749.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586421B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-b8875a936ac846278bef037080a5ef88 |
| Source note | uspto-grants-2003_07 |