HRID1356446

反应详情

EQUATION

反应方程式

HRID 1356446 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

CONDITIONS

反应条件

温度
50 °C

PROCEDURE

实验过程

The mixture of methyl 6-hydroxynicotinate (6 g), 4-biphenylylmethyl bromide (7.7 g), silver carbonate (4.8 g), and toluene (60 ml) was stirred at 50° C. for 12 hr. The reaction mixture was further stirred at 100° C. for 6 hr and filtrated.

WORKUP

后处理

  1. stirringThe reaction mixture was further stirred at 100° C. for 6 hr
  2. filtrationfiltrated