Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1356456Generated: November 2, 2026

HCID 18508351, compound → HCID 18508359, compound

https://huagongshe.com/reaction/1356456

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18508351HCID 18508351—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 18508359HCID 1850835996.4%

Reaction Steps

To a solution of benzyl 4-(2-((2-(dimethylamino)ethyl)(methyl)amino)-2-oxoethyl)phenylcarbamate (0.7 g) in ethanol (10 ml) was added 10% Pd-C (0.2 g). The reaction mixture was hydrogenated under atmospheric pressure at room temperature for one hr. The catalyst was removed by filtration and the filtrate was concentrated to obtain the titled compound (0.43 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06586475B1
Source datasetuspto-grants-2003_07
ORD IDord-af0701dfd6184750b9f027b191a68f09
Source noteuspto-grants-2003_07