HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18508351, compound → HCID 18508359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18508351 | HCID 18508351 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18508359 | HCID 18508359 | 96.4% |
Reaction Steps
To a solution of benzyl 4-(2-((2-(dimethylamino)ethyl)(methyl)amino)-2-oxoethyl)phenylcarbamate (0.7 g) in ethanol (10 ml) was added 10% Pd-C (0.2 g). The reaction mixture was hydrogenated under atmospheric pressure at room temperature for one hr. The catalyst was removed by filtration and the filtrate was concentrated to obtain the titled compound (0.43 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586475B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-af0701dfd6184750b9f027b191a68f09 |
| Source note | uspto-grants-2003_07 |