HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18509283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | N-(4-Methoxy-2-nitrophenyl)-4-methylbenzenesulfonamide | HCID 225676 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18509283 | HCID 18509283 | 83% |
Reaction Steps
To a solution of 4′-Methoxy-2′-nitro-p-toluenesulfonanilide (0.32 g (1.00 mmol)) in pyridine (1,0 ml), p-toluenesulfonyl chloride (0.20 g (1.05 mmol)) was added with stirring at room temperature. After 15 hours' stirring at room temperature, the reaction mixture was poured into water and crystals separated was filtered and washed to give 0.34 g (83%) of the title compound as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586617B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-3f1dbecdb1784d3980671684b12d3491 |
| Source note | uspto-grants-2003_07 |