HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 86759053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-(3-(Bromomethyl)phenyl)ethan-1-one | HCID 15479807 | — |
| Reactant | N,6,6-trimethylhept-2-en-4-yn-1-amine | HCID 53427009 | — |
| Product | HCID 86759053 | HCID 86759053 | 14.8% |
Reaction Steps
The procedure described in Example 1 was repeated, except that N-(6,6-dimethyl-2-hepten-4-ynyl)methylamine (trans:cis=about 3:1) (17.7 g; 116.8 mmol), sodium carbonate (17.7 g; 166.8 mmol), and 3′-bromomethylacetophenone (23.7 g; 111.2 mmol) were used, to thereby yield 4.67 g of the target compound (yield: 14.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586633B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-4e1cbbb16be4414a9fc79c44797deb0f |
| Source note | uspto-grants-2003_07 |