HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 18509452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 1-(3-(Bromomethyl)phenyl)ethan-1-one | HCID 15479807 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18509452 | HCID 18509452 | 69.9% |
Reaction Steps
The procedure described in Referential Example 4 was repeated, except that isopropylamine (instead of triethylamine) (11.82 g; 200 mmol) and 3′-bromomethylacetophenone (4.26 g; 20 mmol) were used, to thereby yield 2.67 g of the target compound (yield: 69.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586633B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-a32234aca39344629654e65ccc48d9fe |
| Source note | uspto-grants-2003_07 |