HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 18509482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 18509452 | HCID 18509452 | — |
| Reactant | 1-Bromo-6,6-dimethylhept-2-en-4-yne | HCID 45489594 | — |
| Product | HCID 18509482 | HCID 18509482 | 61.8% |
Reaction Steps
The procedure described in Example 13 was repeated, except that 3′-(N-isopropylaminomethyl)acetophenone (1.66 g; 8.7 mmol), sodium carbonate (925 mg; 8.7 mmol), and 1-bromo-6,6-dimethyl-2-hepten-4-yne (1.74 g; 8.7 mmol) were used, to thereby yield 1.67 g of the target compound (yield: 61.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586633B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-b280d3dc67704f01a954a4b48bd5fa24 |
| Source note | uspto-grants-2003_07 |