HuagongsheHuagongshe Chemistry Print Report · For research reference only
trans-N-(6,6-Dimethyl-2-hepten-4-ynyl)-N-ethyl-(3-isopropenylbenzyl)amine → trans-N-(6,6-Dimethyl-2-hepten-4-ynyl)-N-ethyl-(3-isopropenylbenzyl)amine Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | trans-N-(6,6-Dimethyl-2-hepten-4-ynyl)-N-ethyl-(3-isopropenylbenzyl)amine | HCID 18509410 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | trans-N-(6,6-Dimethyl-2-hepten-4-ynyl)-N-ethyl-(3-isopropenylbenzyl)amine Hydrochloride | HCID 18509438 | 66.8% |
Reaction Steps
The procedure described in Example 12 was repeated, except that Compound 44 (950 mg; 3.2 mmol) and 4N hydrochloric acid—ethyl acetate solution (0.85 ml; 3.4 mmol) were used, to thereby yield 710 mg of the target compound (yield: 66.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586633B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-a05cfe2a5c1b4f19ab8d1dfc945ef06e |
| Source note | uspto-grants-2003_07 |