HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69991543, compound → HCID 86759058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69991543 | HCID 69991543 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86759058 | HCID 86759058 | — |
Reaction Steps
Meta-(3,5dimethylmorphohno) nitrobenzene (1a) (2 g, 8.5 mmol) is hydrogenated in ethanol (50 ml), over 10%Pd on carbon (200 mg) for 1.5 hours. The catalyst is removed by filtration and the solvent removed evaporation to yield an oil. The enantiomers can be separated by silica column chromatography. ES+ (M+1) 207.36.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06589950B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-bef59b385d6d40c6b03f6a27d75d864b |
| Source note | uspto-grants-2003_07 |