HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18504786, compound → HCID 13931389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18504786 | HCID 18504786 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13931389 | HCID 13931389 | — |
Reaction Steps
The reaction is carried out using an analogous method to (9b), using N-propionyl-N-methyl-4-nitroaniline (10a)(6.8 g, 32.86 mmol), 10%Pd on carbon (447 mg) in THF (75 ml). The hydrogenation yields an oil. ES+ (M+1) 178.87.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06589950B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-d933b64494b546c887d8d9dec84f21ca |
| Source note | uspto-grants-2003_07 |