化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-Benzyloxy-4-methoxybenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Benzyloxy-p-anisic acid | HCID 94057 | — |
| 生成物 | 3-Benzyloxy-4-methoxybenzoyl chloride | HCID 10967795 | 98% |
反応手順
Operating analogously to example 2 starting from 3-benzyloxy-4-methoxy benzoic acid (35.86 g, 0.139 moles) obtained as described in example 1, in thionyl chloride (150 ml), 35.01 g of the title product were obtained (yield: 98%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06589951B1 |
| 出典データセット | uspto-grants-2003_07 |
| ORD ID | ord-fceea9f58b0046dab470beeac4ead0bc |
| 出典メモ | uspto-grants-2003_07 |