HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 18504828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 18504806 | HCID 18504806 | — |
| Product | HCID 18504828 | HCID 18504828 | — |
Reaction Steps
Operating analogously to example 7 staring from 6-methoxy-5-(tetrahydropyran-2-yl-methoxy)-2H-phthalazin-1-one (1.48 g, 5.12 mmoles), obtained as described in example 42, and phosphoryl chloride (6 ml) 1.65 g of the title product as a crude were obtained and used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06589951B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-dcb966d869a04205866ed7871594bf49 |
| Source note | uspto-grants-2003_07 |