HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 18504791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 18504808 | HCID 18504808 | — |
| Product | HCID 18504791 | HCID 18504791 | 88% |
Reaction Steps
Operating analogously to example 7 starting from 6-methoxy-5-(tetrahydro-furan-3-yloxy)-2H-phthalazin-1-one (1.73 g, 6.6 mmoles) and phosphoryl chloride (6.7 ml, 73 mmoles), 1.63 g of the title product were obtained (yield: 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06589951B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-fd6ce255ff3e4ccca234ac553ae3d41e |
| Source note | uspto-grants-2003_07 |