Benzenesulfonyl chloride → HCID 21134139, compound

HRID 1357087Notes

Reaction equation

HRID 1357087 reaction equation
Cl.[NH2:2][CH:3]([C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([O:16][CH3:17])[CH:11]=1)[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6].[C:18]1([S:24](Cl)(=[O:26])=[O:25])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>C(N(CC)CC)C>[C:18]1([S:24]([NH:2][CH:3]([C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([O:16][CH3:17])[CH:11]=2)[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6])(=[O:26])=[O:25])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

4

Reactant 2

HCID 7369Benzenesulfonyl chlorideHCID 18505407210161-73-2

Product 1

HCID 21134139HCID 21134139, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Corresponding to Example 1c, 10 g of (8b) were treated with phenylsulphonyl chloride and triethylamine. A yellowish solid was obtained (yield: 13.2 g).

Workup

  1. customA yellowish solid was obtained (yield: 13.2 g)

Sources & evidence

ORD record
ord-1ead2670b1ba4396aef1d59c02626a13
Source dataset
uspto-grants-2003_07
Patent number
US06589972B2

Reaction notes

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