Lithium Hydroxide → HCID 178512492, compound

HRID 1357090Notes

Reaction equation

HRID 1357090 reaction equation
[C:1]1([S:7]([NH:10][CH:11]([C:17]2[CH:22]=[CH:21][CH:20]=[C:19]([O:23][CH2:24][C:25]3[CH:30]=[CH:29][CH:28]=[C:27]([NH:31][C:32]([NH2:34])=[NH:33])[CH:26]=3)[CH:18]=2)[CH2:12][C:13]([O:15]C)=[O:14])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Li+]>>[C:1]1([S:7]([NH:10][CH:11]([C:17]2[CH:22]=[CH:21][CH:20]=[C:19]([O:23][CH2:24][C:25]3[CH:30]=[CH:29][CH:28]=[C:27]([NH:31][C:32]([NH2:34])=[NH:33])[CH:26]=3)[CH:18]=2)[CH2:12][C:13]([OH:15])=[O:14])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 3939Lithium HydroxideHCID 178500870HCID 178500870, compound

Product 1

HCID 178512492HCID 178512492, compound

Procedure

Corresponding to Example 4g, 471 mg of (8h) were hydrolysed using lithium hydroxide. A white solid was obtained (yield: 253 mg).

Workup

  1. customA white solid was obtained (yield: 253 mg)

Sources & evidence

ORD record
ord-a29729c9ebb2430f85bea1ae0db141c8
Source dataset
uspto-grants-2003_07
Patent number
US06589972B2

Reaction notes

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