Ammonium Hydroxide → HCID 18506197, compound

HRID 1357372Notes

Reaction equation

HRID 1357372 reaction equation
[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[C:10](=[O:14])[NH:9][C:8]2=[O:15].[OH-].[NH4+:21]>>[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]([C:8]([NH2:21])=[O:15])[C:11](=[CH:12][CH:13]=1)[C:10]([NH2:9])=[O:14]

Participants

3

Reactant 2

HCID 14923Ammonium HydroxideHCID 18506076HCID 18506076, compound

Product 1

HCID 18506197HCID 18506197, compound

Procedure

5-(2-Aminophenoxy)-isoindole-1,3-dione (0.1 g, 0.38 mmol) in conc. ammonium hydroxide (aq) was stirred at 60° C. for two hours. The reaction mixture was evaporated in vacuo (cold in order not to make the imide again). The crude mixture was used without any purification.

Workup

  1. customThe reaction mixture was evaporated in vacuo (cold in order not
  2. customThe crude mixture was used without any purification

Sources & evidence

ORD record
ord-fc642962978f4fe8bbdcf534f802d180
Source dataset
uspto-grants-2003_07
Patent number
US06590118B1

Reaction notes

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