HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 91616889, compound → HCID 90829811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 91616889 | HCID 91616889 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 90829811 | HCID 90829811 | — |
Reaction Steps
PCC/Al2O3 can be added to a room temperature solution of Example 13L in dichloromethane. After stirring overnight, the reaction mixture can be filtered and concentrated. The concentrate can be purified by flash chromatography using ethyl acetate to afford the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593314B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-17ef4c164ef64ed1ac641cd7b72bf50d |
| Source note | uspto-grants-2003_07 |