Potassium Carbonate → HCID 59076541, compound

HRID 1357513Notes

Reaction equation

HRID 1357513 reaction equation
C(=O)([O-])[O-].[K+].[K+].C([O:15][C@@H:16]1[CH2:21][C@@:20]([OH:26])([C:22]([O:24][CH3:25])=[O:23])[CH2:19][C@@H:18]([CH:27]=[CH2:28])[C@@H:17]1[OH:29])(=O)C1C=CC=CC=1>CO>[OH:26][C@:20]1([C:22]([O:24][CH3:25])=[O:23])[CH2:19][C@@H:18]([CH:27]=[CH2:28])[C@H:17]([OH:29])[C@H:16]([OH:15])[CH2:21]1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 70020327HCID 70020327, compound

Product 1

HCID 59076541HCID 59076541, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Potassium carbonate can be added to a room temperature solution of Example 17E in methanol. After stirring for 1 hour, the reaction mixture can be filtered, and concentrated. The concentrate can be purified by flash chromatography to afford the desired product.

Workup

  1. filtrationthe reaction mixture can be filtered
  2. concentrationconcentrated
  3. concentrationThe concentrate can
  4. custombe purified by flash chromatography

Sources & evidence

ORD record
ord-999285e23a024ba887c7d75eb21594ba
Source dataset
uspto-grants-2003_07
Patent number
US06593314B1

Reaction notes

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