HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 131723975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 59076541 | HCID 59076541 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131723975 | HCID 131723975 | — |
Reaction Steps
Thionyl chloride can be added dropwise to a 0° C. solution of Example 17F and triethylamine in dichloromethane. After stirring for 30 minutes, the reaction mixture can be washed with saturated NaHCO3 solution, and brine, dried (MgSO4) filtered and concentrated to afford the crude desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593314B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-ddd6e50730c24dbba600a78129067b7e |
| Source note | uspto-grants-2003_07 |