HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 91569368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 131723976 | HCID 131723976 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 91569368 | HCID 91569368 | — |
Reaction Steps
Methanesulfonyl chloride can be added dropwise to a 0° C. solution of Example 13H and triethylamine in dichloromethane. The reaction mixture can be stirred for 2 hours, washed with saturated NaHCO3 solution, brine, dried (MgSO4), filtered and concentrated. The concentrate can be purified by flash chromatography to afford the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593314B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-6f475ed5d2df43788bb37efc5cfbb0db |
| Source note | uspto-grants-2003_07 |