Sodium hydride → HCID 18186829, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure of example 4, step 1 starting from 2,6-dichloropyrazine (444 mg, 3.00 mmol) and 4-trifluoromethylbenzyl alcohol (581 mg, 3.30 mmol) and NaH (55% in mineral oil, 144 mg, 3.30 mmol). Recrystallization from hexane gave 0.81 g (93%) of the title compound: mp 67-69° C. MS m/z 289 (M+H)+. Anal. (C12H8ClF3N2O) C, H, N.

Provenance & Evidence