Ethylene carbonate → HCID 18186793, compound

HRID 1357634Notes

Reaction equation

HRID 1357634 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([OH:13])[CH:7]=[CH:6]2.C1(=O)O[CH2:17][CH2:16][O:15]1>CO.C(Cl)(Cl)Cl.CCCCCC>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([O:13][CH2:17][CH2:16][OH:15])[CH:7]=[CH:6]2

Participants

4

Reactant 2

HCID 7303Ethylene carbonateHCID 2886346-Methoxy-2-naphthol

Product 1

HCID 18186793HCID 18186793, compound

Reagents, catalysts & solvents 1

HCID 22285155HCID 22285155, compoundSolvent

Procedure

*Prepared from 6-methoxy-2-naphthol and ethylene carbonat according to the procedure of Example 134, step 1, in WO 00/76984. The reaction mixture was refluxed for 2 h. Pure 2-(6-methoxy-naphthalen-2-yloxy)ethanol was obtained by recrystallization from MeOH/CHCl3/n-hexane.

Workup

  1. temperatureThe reaction mixture was refluxed for 2 h

Sources & evidence

ORD record
ord-414f885c9df546a7866e1c4dbb3a2be7
Source dataset
uspto-grants-2003_07
Patent number
US06593330B2

Reaction notes

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