HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 18187426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 18187410 | HCID 18187410 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18187426 | HCID 18187426 | — |
Reaction Steps
Batch size: 11.5 g (27.4 mmol) 2-{4-[4-(2-oxo-2,3-dihydro-benzoimidazol-1-yl)-piperidin-1-yl]-butyl}-isoindolin-1,3-dione and 2.7 ml (55 mmol) hydrazine.hydrate in 60 ml ethanol. The accumulated crude product is further processed without further purification: Yield 5.1 g (64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593344B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-b90cb24195e04d77bb404dcc919c6283 |
| Source note | uspto-grants-2003_07 |