HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178424777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 178424888 | HCID 178424888 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 178424777 | HCID 178424777 | 162.8% |
Reaction Steps
0.13 g (0.4 mmol) of 1′,2′,3′,4′,5′-pentamethylferrocene-1-carboxylic acid azide are stirred with 0.5 ml of acetic acid in 10 ml of acetic anhydride at 80° c for five hours. Aqueous work-up gives 0.102 g of 1′,2′,3′,4′,5-pentamethylferrocen-1-yl-acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593437B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-6ee2614fb0f6436994b5253b706e2552 |
| Source note | uspto-grants-2003_07 |