HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzenesulfonic acid → HCID 18504111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | HCID 18188678 | HCID 18188678 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18504111 | HCID 18504111 | — |
Reaction Steps
A solution of Example 27E (4.1 g, 8.3 mmol) and toluenesulfonic acid (1 g, 5.2 mmol) in methanol (100 mL) was stirred for 1 hour, and reduced in volume under reduced pressure. The solid was then collected by filtration to provide the titled compound. MS(ESI(−)Q1MS) m/z 504 and 506 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593480B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-112309af8c7646b3bbb5dc2dcc2471b0 |
| Source note | uspto-grants-2003_07 |