HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 88064075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 88063986 | HCID 88063986 | — |
| Product | HCID 88064075 | HCID 88064075 | — |
Reaction Steps
A suspension of the compound obtained in Step E (1.26 g, 3.0 mmol) in 18 ml of 28 % ammonium hydroxide is stirred. After a few minutes, dissolution is observed. Stirring is continued for 30 minutes and the reaction mixture is acidified with 4N HCl. A few ml of ethyl acetate are added, with stirring, and precipitation is produced. The precipitate is filtered off and dried in vacuo to yield the title product in the form of cream-coloured powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596709B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-63a37cb39a7d42b68be35195f31c8f47 |
| Source note | uspto-grants-2003_07 |