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HRID1358228

反应详情

EQUATION

反应方程式

HRID 1358228 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：Nc1nc2c(c(=O)[nH]1)NC(CNc1ccc(C(=O)N[C@@H](CCC(=O)O)C(=O)O)cc1)CN2
HCID135444742

Tetrahydrofolic acid

C19H23N7O6

PRODUCTS

生成物

1
结构：Nc1nc2c(c(=O)[nH]1)N[C@H](CNc1ccc(C(=O)N[C@@H](CCC(=O)O)C(=O)O)cc1)CN2
HCID135415876

未命名化合物

PROCEDURE

实验过程

One half of the mother liquor is precipitated with 1.1 g of ethanol, giving enriched amorphous (6R) tetrahydrofolic acid with a chemical content of 63.3% and a (6R) percentage of 75.9, while in the other half of the mother liquor the pH is rapidly brought to 3.5 using 6.3 g of hydrochloric acid, resulting in enriched, amorphous (6R)-tetrahydrofolic acid with a chemical content of 64.8% and a (6R) percentage of 75.9.

WORKUP

后处理

  1. customOne half of the mother liquor is precipitated with 1.1 g of ethanol
  2. customgiving enriched amorphous (6R) tetrahydrofolic acid with a chemical content of 63.3%