2-Amino-5-methylpyridine → HCID 622689, compound

HRID 1358252Notes

Reaction equation

HRID 1358252 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([NH2:8])=[N:6][CH:7]=1.Br[CH2:10][C:11]([C:13]1[CH:18]=[CH:17][C:16]([O:19][CH3:20])=[C:15]([O:21][CH3:22])[CH:14]=1)=O>>[CH3:22][O:21][C:15]1[CH:14]=[C:13]([C:11]2[N:8]=[C:5]3[CH:4]=[CH:3][C:2]([CH3:1])=[CH:7][N:6]3[CH:10]=2)[CH:18]=[CH:17][C:16]=1[O:19][CH3:20]

Participants

3

Reactant 2

HCID 153482-Amino-5-methylpyridineHCID 2704232-Bromo-1-(3,4-dimethoxyphenyl)ethan-1-one

Product 1

HCID 622689HCID 622689, compound

Procedure

The title compound, MS: m/e=269.2 (M+H+), was prepared in accordance with the general method of example 8 from 5-methyl-pyridin-2-ylamine and 2-bromo-1-(3,4-dimethoxy-phenyl)-ethanone.

Sources & evidence

ORD record
ord-480b860903f246d5b8bcdfa64dc5c302
Source dataset
uspto-grants-2003_07
Patent number
US06596731B2

Reaction notes

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