Cyclopentanol → HCID 54561802, compound
Reaction equation
[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:19]1([OH:24])[CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH:19]1([O:24][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH2:23][CH2:22][CH2:21][CH2:20]1Participants
3
Procedure
The title compound, white solid, m.p. 120-123° C. and MS: m/e=323.4 (MH+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and cyclopentanol.
Sources & evidence
- ORD record
- ord-d34b5c9914a443bfa35949fd04b9d682
- Source dataset
- uspto-grants-2003_07
- Patent number
- US06596743B2
Reaction notes
Loading…