2,2,2-Trifluoroethanol → HCID 11078236, compound

HRID 1358408Notes

Reaction equation

HRID 1358408 reaction equation
[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[F:19][C:20]([F:24])([F:23])[CH2:21][OH:22]>>[F:19][C:20]([F:24])([F:23])[CH2:21][O:22][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 64092,2,2-TrifluoroethanolHCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 11078236HCID 11078236, compound

Procedure

The title compound, white solid, m.p.=125-127° C. and MS: m/e=337.3 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and 2,2,2 trifluoro-ethanol.

Sources & evidence

ORD record
ord-ad315ca742484b43a8027f9e4293c199
Source dataset
uspto-grants-2003_07
Patent number
US06596743B2

Reaction notes

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