HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2-(3,4-Dichlorophenyl)acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3,4-Dichlorophenylacetic acid | HCID 79874 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-(3,4-Dichlorophenyl)acetyl chloride | HCID 2758149 | 100% |
Reaction Steps
A solution of (3,4-dichloro-phenyl) acetic acid (3.51 g, 0.0179 mol) and oxalyl chloride (17.5 g, 12.08 mL, 0.089 mol) in 150 mL of benzene was refluxed for 6 h. The solution was evaporated with benzene 3 times and dried in vacuum. Yield 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596734B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-c5bf20ff8c2c490ca43a4fe15379f5eb |
| Source note | uspto-grants-2003_07 |