HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 9809980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 9896275 | HCID 9896275 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9809980 | HCID 9809980 | 60.3% |
Reaction Steps
Reaction and isolation were conducted in a similar procedure to that described in Example 2 using methyl 3-[4-[6-(3,5-di-t-butyl4-hydroxyphenylthio)-1-methyl-1H-benzimidazol-2-ylmethoxy]phenyl]-2-(4-fluorobenzyloxy)propionate (0.22 g), aqueous 2N sodium hydroxide solution (2 ml) and methanol (5 ml) to afford the title compound (0.13 g, mp 40-46° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596751B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-808b9a0870944ed796b3defabaf88224 |
| Source note | uspto-grants-2003_07 |