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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1358563Generated: October 31, 2026

Sodium Hydroxide → HCID 9809980, compound

https://huagongshe.com/reaction/1358563

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 9896275HCID 9896275—
SolventMethanolHCID 887—
ProductHCID 9809980HCID 980998060.3%

Reaction Steps

Reaction and isolation were conducted in a similar procedure to that described in Example 2 using methyl 3-[4-[6-(3,5-di-t-butyl4-hydroxyphenylthio)-1-methyl-1H-benzimidazol-2-ylmethoxy]phenyl]-2-(4-fluorobenzyloxy)propionate (0.22 g), aqueous 2N sodium hydroxide solution (2 ml) and methanol (5 ml) to afford the title compound (0.13 g, mp 40-46° C.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06596751B2
Source datasetuspto-grants-2003_07
ORD IDord-808b9a0870944ed796b3defabaf88224
Source noteuspto-grants-2003_07