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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1358664Generated: October 31, 2026

HCID 21893489, compound → HCID 11381315, compound

https://huagongshe.com/reaction/1358664

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21893489HCID 21893489—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 11381315HCID 1138131599.4%

Reaction Steps

A solution of 0.024 g (0.078 mmol) of material from Example 130 and 5 mg 5% palladium on carbon in 5 mL ethyl acetate was degassed three times under a hydrogen balloon and stirred at room temperature for 4 hr. The mixture was filtered and concentrated in vacuo. The residue was recrystallized from ether and hexane to afford 0.024 g (99%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06596716B2
Source datasetuspto-grants-2003_07
ORD IDord-dc662a6ceef44c95808beb2497c7d879
Source noteuspto-grants-2003_07