HCID 87924367, compound → HCID 87924368, compound

Participants

Reaction Steps

1,2-bis(4-trifluoromethylthiophenyl)acetylene (200 mg, 0.53 mmol) was hydrogenated over 10% palladium on carbon (20 mg) in hexane (30 mL) at rt for 2 hours. The reaction was filtered and the filtrate was concentrated to give 0.21 g (100%) of 1,2-bis(4-trifluoromethylthiophenyl)ethane. 1HNMR (360 MHz, DMSO-d6) δ 7.61 (d, J=8.3 Hz, 4H), 7.40 (d, J=8.3 Hz, 4H), 2.97 (s, 4H, CH2CH2). MS-EI m/z 382 [M+].

Provenance & Evidence